Flash spark plasma sintering of pure TiB2

Flash (Ultra-Rapid) Spark-Plasma Sintering of Silicon Carbide

A new ultra-rapid process of flash spark plasma sintering is developed. The idea of flash spark plasma sintering (or flash hot pressing - FHP) stems from the conducted theoretical analysis of the role of thermal runaway phenomena for material processing by flash sintering. The major purpose of the present study is to theoretically analyze the thermal runaway nature of flash sintering and to exp...

Microstructure of spark plasma sintered TiB2 and TiB2–AlN ceramics

In this research study, the effects of aluminum nitride (AlN) additive on the densification behavior and microstructure development of titanium diboride (TiB2) based ceramic matrix composite were investigated. In this way, a monolithic TiB2 ceramic and a TiB2–5 wt% AlN ultrahigh temperature ceramic composite were fabricated by spark plasma sintering (SPS) proces...

Ultrafast-Contactless Flash Sintering using Plasma Electrodes

This paper presents a novel derivative of flash sintering, in which contactless flash sintering (CFS) is achieved using plasma electrodes. In this setup, electrical contact with the sample to be sintered is made by two arc plasma electrodes, one on either side, allowing current to pass through the sample. This opens up the possibility of continuous throughput flash sintering. Preheating, a usua...

Spark Plasma Sintering of Negative Temperature Coefficient Thermistor Ceramics

Application of Spark Plasma Sintering for Manufacturing of Thermoelectric Materials

V-VI thermoelectric compounds like Bi2Te3-based alloys are well known for room temperature applications like Peltier coolers or thermogenerators. Their anisotropic physical properties and mechanical weakness are a problem for the manufacturing. To overcome the mechanical problem Spark Plasma Sintering (SPS) was used. 2 inch Wafers of polycrystalline bismuth telluride based n-type and p-type the...